HomeMy WebLinkAboutAppendix A Soil Laboratory ReportsAPPENDIX A
SOIL LABORATORY REPORTS
Black Diamond Resorts LLC ATCAssociates bic.
Vail, Colorado
'gle 0�
Report To:
ATC Associates, Inc,
Chris Woods
8985 E. Nichols Ave. Suite 350
Centennial
CO
80112 -
ph: (303) 799 -6100 tax:
D'Anna Stelly
Project Manager
ATC Associates, Inc.
Certificate of Analysis Number:
07030504
Project Name:
Site:
Site Address:
PO Number:
State:
State Cert. No.:
Date Reported:
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Vail
Centennial, CO
Colorado
311512007
This Report Contains A Total Of 31 Pages
Excluding This Page
VMS
Chain Of Custody
3/15/2007
Date
O
Report To:
ATC Associates, Inc.
Chris Woods
8985 E. Nichols Ave. Suite 350
Centennial
CO
80112 -
ph: (303) 799 -6100 fax:
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Case Narrative for:
ATC Associates, Inc.
Certificate of Analysis Number:
07030504
Proiect Name:
Site:
Site Address:
PO Number:
State:
State Cent. No.:
Date Reported:
Vail
Centennial, CO
Colorado
3/1512007
Results are reported on a wet weight basis unless dry- weight correction is denoted in the units field on the analytical report (" mglkg•dry " or
uglkg -dry „ ).
Matrix spike (MS) and matrix spike duplicate (MSD) samples are chosen and tested at random from an analytical batch of "like" matrix to
check for possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the
laboratory. Since the MS and MSD are chosen at random from an analytical batch, the sample chosen for spike purposes may or may not
have been a sample submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this
analytical report is determined by the Laboratory Control Sample (LCS) and the Method Blank (MB). The Laboratory Control Sample (LCS)
and the Method Blank (MB) are processed with the samples and the MS /MSD to ensure method criteria are achieved throughout the entire
analytical process.
Some of the percent recoveries and RPD's on the QC report for the MS /MSD may be different than the calculated recoveries and RPD's
using the sample result and the MS /MSD results that appear on the report because, the actual raw result is used to perform the calculations
for percent recovery and RPD.
Any other exceptions associated with this report will be footnoted in the analytical result page(s) or the quality control summary page(s).
Please do not hesitate to contact us if you have any questions or comments pertaining to this data report. Please reference the above
Certificate of Analysis Number.
This report shall not be reproduced except in full, without the written approval of the laboratory. The reported results are only representative
of the samples submitted for testing.
SPL, Inc. is pleased to be of service to you. We anticipate working with you in fulfilling all your current and future analytical needs
D'Anna Stelly
Project Manager
07030504 Page
311512007
Date
Test results meet all requirements of NELAC, unless specified in the narrative.
O
ATC Associates, Inc.
Certificate of Analysis Number:
07030504
Report To: ATC Associates, Inc.
Chris Woods
8985 E. Nichols Ave. Suite 350
Centennial
CO
80112-
ph: (303) 799 -6100 fax: (303) 799 -3441
Fax To:
Project Name:
Site:
Site Address:
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Vail
Centennial, CO
PO Number:
State: Colorado
State Cert. No.:
Date Reported: 3/15/2007
Client Sample ID
'EXC -1 -10
EXC-1 -20'
_
;EXC -1 -25'
EXC -2 -10'
'EXC -2 -20'
EXC -2 -25'
jEXC -3 10'
Lab Sample ID
07030504-01
1 07030504 -02
—
Matrix
Soil
_....._. _ ...._ ......
Date Collected
... - -- --
Date Received
COC ID
HOLD
3/8/2007 3:00:00 PM
3/10/2007 10:00:00 AM
221042
---2-21-0--4'2-- - ._..
.-[
Soil
3/8/2007 3:15:00 PM
3/8/2007 3:30:00 PM
3/10/2007 10:00:00 AM
3/1012007 10:00:00 AM
07030504 -03
07030504 -04
Soil
221042
Soil
3/8/2007 4:15:00 PM
3/8/2007 4:30:00 PM
3/10/2007 10:00:00 AM
3/10/2007 10:00:00 AM
221042
El
07030504 -05
07030504-06
Soil
221042
El
Soff
3/8/2007 4:40:00 PM
3/10/2007 10:00:00 AM
3/10/2007 10:00:00 AM
221042
221042
07030504 -07
Soil
3/8/2007 5:00:00 PM
D'Anne Stelly
Project Manager
Joel Grice
Laboratory Director
Ted Yen
Quality Assurance Officer
3/15/2007
Date
07030504 Page 2
3/15/2007 11:01:01 AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -10' Collected: 03/08/2007 15:00 SPL Sample ID: 07030504 -01
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limlt D11. Factor Date Analyzed Analyst Seq. #!
DIESEL RANGE ORGANICS MCL CO_DRO Units: mglkg -dry
Diesel Range Organics, C11- C28 1.2 J 0.71 15 1 03/11/07 21:20 NW 3715873
Surr. n- Pentacosane 108 0 % 20 -154 1 03/11/07 21:20 NW 3715873
Prep Method Prep Date Prep Initials Prep Factor
SW3550B 03/10/200715:31 Pr
1.00
D'Anna Stelly
Project Manager
Qualifiers:
ND /U - Not Detected at the Method Detection Limit
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
- Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 3
B - Analyte detected in the associated Method Blank above Rep.Limit 311512007 11:01,13 AM
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportabie due to Dilution
MI - Matrix Interference
- Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 4
B - Analyte detected in the associated Method Blank above Rep.Limit 311512007 11:01:13 AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
®
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -10'
Collected: 03/08/2007 15:00 SPL Sample ID: 07030504 -01
Site: Centennial, CO
Analyses /Method Result QUAL
MDL Rep.Limlt
DII. Factor Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS BY METHOI? 82608
MCL
SW8260B Units: uglkg -dry
Benzene ND
0.1
5.1
1
03/13/0711:41 DY
3718743
Ethylbenzene ND
0.14
5.1
1
03/13/0711:41 DY
3718743
Gasoline Range Organics _ND
9.9
51
1
03/13/07 11:41 DY
3718743
Toluene ND
0.18
5.1
1
03/13/0711:41 DY
3718743
Xylenes,Total ND
6.16
5.1
1
03113/0711:41 DY
3718743
Surr: 1,2- Dichloroethane -d4 93.5i
0
% 41 -155_
1
03/13/0711:41 DY
3718743
Surr:4- Bromofluorobenzene u 97.5
0
% -64 -147
1
03!13/0711:41 DY_
3718743
Surr: Toluene -d8 101
0
% 52 -152
1
03/13/07 11:41 DY
3718743
Preo Method Preo Date pre lnitials
Preo Factor
SW50308 03/12/200715:31 IDY
11.00
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportabie due to Dilution
MI - Matrix Interference
- Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 4
B - Analyte detected in the associated Method Blank above Rep.Limit 311512007 11:01:13 AM
lP
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -10' Collected: 03/08/2007 15:00 SPL Sample ID: 07030504 -01
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limlt Dit. Factor Date Analyzed Analyst Seq. #
PERCENT MOISTURE MCL D2216 Units: wt%
Percent Moisture 2.79 0 0 1 03/10107 12:17 T L 3714717
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit
J - Estimated Value between MDL and PQL
* - Surrogate Recovery Outside Advisable QC Limits
>MCL - Result Over Maximum Contamination Limit(MCL
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument
B - Analyte detected in the associated Method Blank above Rep.Limit
07030504 Page 5
3115/2007 11:01:14 AM
O
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -20' Collected: 03/08/2007 15:15 SPL Sample ID: 07030504 -02
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit Dil. Factor Date Analyzed Analyst Seq. #
DIESEL RANGE ORGANICS MCL C_O_DRO Units: mglkg -dry
Diesel Range Organics, C11- C28 ND 0.88 19 u 1 03/11107 22:28 NW 3715876
Surr: n- Pentacosane 92.5 _ 0 % 20 -154 1 03/11/07 22:28 NW 3715876
Prep Method Prep Date Prep Initials Prep Factor
SW3550B 03110/200715:31 JJDM 1.00
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matra Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 6
B - Analyte detected in the associated Method Blank above Rep.Limit 3/1512007 11:01:14 AM
A ZOW
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -20' Collected: 03/0812007 15:15 SPL Sample ID: 07030504 -02
Site: Centennial, CO
Analyses /Method R
Result QUAL M
MDL R
Rep.Limit D
Dil. Factor Date Analyzed A
Analyst S
Seq. #
VOLATILE ORGANICS BY METHOD 8260B M
MCL SW8260B Units: u
ug /kg -dry
Benzene N
NO 0
0.13 6
6.4 1
1 03/13/0712:03 D
DY 3
3718744
Ethylbenzene 0
0.5 J 0
0.17 6
6.4 1
1 03/13/0712:03 D
DY 3
3718744
..... .
......-- - - - -
-... - ....._..__._.. -
-- .. — ._.._. ..
Xylenes,Total
Surr: 1,2- Dichioroethane -d4
Surr: 4- Bromofluorobenze n e
Surr: Toluene -d8
0 -87 J 0.2
6.4 1 03113/0712:03 DY 3718744
93.5 41 -155
94.9 0 °h 64 -147
104 0 % 52 -152
Prep Method Prep Date Prep Initials Prep Factor
SW50308 03/12/200715:33 DY 1.00 1
1 03/13/0712:03 DY 3718744
1 03/13/0712:03 DY 3718744
1 03/13/0712:03 DY 3718744
D'Anna Steily
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limlt(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matra Interference
- Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 7
B - Analyse detected in the associated Method Blank above Rep.Limit 31151200711:Oi:14AM
ll�
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -20' Collected: 03/08/2007 15:15 SPL Sample ID: 07030504 -02
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit DII. Factor Date Analyzed Analyst Seq. #
PERCENT MOISTURE MCL D2216 Units: wt %a
Percent Moisture 21.7 0 0 1 03/10/0712 :17 T_L 3714716
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC -Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 8
B - Analyte detected in the associated Method Blank above Rep.Limit 3/15/2007 11:01!15 AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
A zl� �� MA ® HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -25' Collected: 03/0812007 15:30 SPL Sample ID: 07030504 -03
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit 1071. Factor Date Analyzed Analyst Seq. #
DIESEL RANGE ORGANICS MCL CO_DRO Units: mglkg -dry
Diesel Range Organics, C11- C28 ND 0.73 16 1 03/11/07 22:51 NW 3715877
Surr: n Pentacosane 102 0 % 20 -154 1 03/11/07 22:51 NW 3715877
Prep Method Prep Date Prep Initials Prep Factor
SW3550B 03/101200715:31 JJDM 111.00
x-') - a..K�
D'Anna Steily
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 9
B - Analyte detected in the associated Method Blank above Rep.Limit 311512007 11:01:16 AM
JR�ro,- AF P_
!;rw�ld 17)
;?0W
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -25' Collected: 03108/2007 15:30 SPL Sample ID: 07030504 -03
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit DII. Factor Date Analyzed Analyst Seq. #
VOLATILE ORGANICS BY METHOD 8260B
Benzene — ND
MCL SW8260B Units: ug /kg -dry
0.11 5.3 1 03/1310712:25 DY 3718745
Ethylbenzene
ND
0.15
5.3
1
03113/0712:25
DY
3718745
Gasoline Range Organics
-
ND
_ --
10
- - - -- - --
53
- --
1
- -- ---------------
03113/0712:25
DY
--
3718745
Toluene
NO
0.18
5.3
1
03/1310712:25
DY
3718745
Xylenes,Total
ND
0.17
__._...._..
5.3
-_ .................................
1
........................__.....
03113/0712:25
DY
-
3718745
Surr:1,2- Dichloroethane -d4
__ ............
95.7
0
% 41 -155
1
03/13/0712:25
DY
3718745
. .. �_ —.... - —
Surr:4- Bromofluorobenzene
97.4
0
% 64 -147
1
03113/0712:25
DY
3718745
Surr: Toluene -d8
104
0
% 52 -152
1
03113107 12:25
DY
3718745
Preo Method IPrea Date Prep Initials Prep Factor
SW5030B 03/121200715:35
DY
1.00
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
Surrogate Recovery Outside Advisable QC Limits TNTC -Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 10
B - Analyte detected in the associated Method Blank above Rep.Limit 3115120071101:16 AM
I
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -1 -25' Collected: 03/08/2007 15:30 SPL Sample ID: 07030504 -03
Analyses /Method
PERCENT MOISTURE
Percent Moisture
Site: Centennial, CO
Result QUAL MDL Rep.Limit DII. Factor Date Analyzed Analyst Seq. #
MCL D2216 Units: wt%
5.8 0 0 1 03/10/0712:17 T_L 3714715
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Umit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
' - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 11
B - Analyte detected in the associated Method Blank above Rep.Limit 3r16r200711:o1:16AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
, zm� Z M Mc® HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -10' Collected: 03/08/2007 16:15 SPL Sample ID: 07030504 -04
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit Dli. Factor Date Analyzed Analyst Seq. #
DIESEL RANGE ORGANICS MCL CO�DRO Units: rggikS ry
Diesel Range Organics, C11- C28 0.75 J 0.72 16 1 03/11/07 23:14 NW 3715878
Surr: n- Pentacosane 99.1 0 % 20 -154 1 03/11/07 23:14 NW 3715878
CPreo Mod Prep Date PreD Initials Prep
Facto
[SW35508 03/10/2D0715:31 JDM x1.00
J-,) - -
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportabie due to Dilution
MI - Matrix Interference
- Surrogate Recovery Outside Advisable QC Limits TNTC -Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 12
8 - Analyte detected in the associated Method Blank above Rep.Limit 3115=07 11.01:17 AM
p
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713)660.0901
Client Sample ID EXC -2 -10'
Collected: 03/08/2007 16:15 SPL Sample ID: 07030504 -04
Site: Centennial, CO
Analyses /Method
Result
QUAL MDL Rep.Limit DII. Factor Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 8260B
MCL
SW8260B Units: ug /kg -dry
Benzene
J NO
0.11
5.2
1 03/13/0712:47 DY
3718746
Ethylbenzene
ND
0.14
5.2
1 03/13/0712:47 DY
3718746
Gasoline Range Organics
ND
10
52
1 03M3107 12:47 DY
3718746
Toluene
ND
0.18
5.2
1 03/13/0712:47 DY
3718746
Xylenes,Total
ND
0.16
5.2
1 03113/0712:47 DY
3718746
Surr :1,2- Dichloroethane -d4
95.1 ��
_
— 0
°% 41 -155
1 03/1310712:47 DY
3718746
Surr:4- Bromofluorobenzene
95.1
0
% 64 -147
1 03/13/0712:47 DY
3718746
Surr. Toluene -d8 101
(Prep Method Prep Date
SW50306 03/12/200715:37
0
jPrev Initials
IDY
% 52 -152
jPrep Factor
11.00
1 03/13/07 12:47 DY
3718746
,
D'Anna Steliy
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
" - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 13
B - Analyse detected in the associated Method Blank above Rep.Limit 311612007 11:01:17 AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
® HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -10' Collected: 03/08/2007 16:15 SPL Sample ID: 07030504 -04
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit DII. Factor Date Analyzed Analyst Seq. #
PERCENT MOISTURE MCL D2216 Units: wt%
_
. . - --
Percent Moisture 3.96 0 0 1 03/10/0712:17 T L 3714714
jc) ' 6L'- �
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
Ml - Matrix Interference
- Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 14
B - Analyte detected in the associated Method Blank above Rep.Limit 3115/2007 11:01:17 AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
060 ow'.® HOUSTON, TX 77054
'ZA (713} 660 -0901
Client Sample ID EXC -2 -20' Collected: 03/08/2007 16:30 SPL Sample ID: 07030504 -05
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit Dil. Factor Date Analyzed Analyst Seq. #
DIESEL RANGE ORGANICS MCL CO DRO Units: mglkg -dry
Diesel Range Organics, C11- C28 0.88 J 0.74 16 1 03/11/07 23:37 NW 3715879
Surr: n- Pentacosane 107 0 % 20 -154 1 03/11/07 23:37 NW 3715879
Prep Method jPrep Date rep Inifials Prep Factor
SW3550B 03/101200715:31 JDM 11.00
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
" - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 15
B - Analyte detected in the associated Method Blank above Rep.Limit 311612007 11:01:18 AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
® HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -20' Collected: 03/08/2007 16:30 SPL Sample ID: 07030504 -05
Site: Centennial, CO
Analyses /Method
Result QUAL
MDL
Rep.Llmit
Dil. Factor Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 82608
MCL
S 260 Units: uglkg -dry
Benzene
ND
0.11
5.3
1
03/13/0713:09
DY
_`_
3718747
Ethylbenzene
ND
0.15
5.3
1
03/1310713:09
DY
3718747
Gasoline Range Organics
ND
10
53
1
03/13/07 13:09
DY
3718747
Toluene
ND
0.18
5.3
1
03113/0713:09
DY
3718747
Xylenes,Total
ND
0.17
5.3
1
03/13/0713 :09
DY
3718747
Surr: 1,2- Dichloroethane -d4
93.8
0
% 41 -155
1
03/13/0713:09
DY
3718747
Surr:4- Bromofluorobenzene 95.0 _ 0 % 64 -147 1 03/13/0713:09 DY 3718747
Surr: Toluene -d8 100 0 % 52 -152 1 03/13/0713:09 DY 3718747
Prep Method Pre Date Prep Initials I� reD Factor
SW5030B 03/12/200715:38 DY �1.00
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
' - Surrogate Recovery Outside Advisable QC Limits TNTC -Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 16
B - Analyse detected in the associated Method Blank above Rep.Limit 3/15/2007 11:01:18 AM
zm� �' MA C�o
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -20' Collected: 03/08/2007 16:30 SPL Sample ID: 07030504 -05
Site: Centennial, CO
Analyses/Method Result QUAL MDL Rep.Limit Dil. Factor Date Analyzed Analyst Seq. #
PERCENT MOISTURE MCL D2216 Units: wt%
Percent Moisture 6.39 0 0 1 03/10/07 12:17 T_L 3714713
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit (MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
` - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 17
B - Analyte detected in the associated Method Blank above Rep.Limit 3/1512007 11:01:19 AM
)�::). 6L-"� --
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 18
B - Analyse detected in the associated Method Blank above Rep.Limit 311612a0711:01:19AM
HOUSTON LABORATORY
zm� Z' 2r®
8880 INTERCHANGE DRIVE
I M
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -25'
Collected: 03/08/2007 16:40 SPL Sample ID: 07030504 -06
Site: Centennial, CO
AnalysesfMethod Result
QUAL MDL Rep.Limit Dil. Factor Date Analyzed Analyst Seq. #
DIESEL RANGE ORGANICS
MCL_
CO_DRO Units: mg1kg-dry _
Diesel Range Organics, C11- C28 0.87
J 18 1
03112/07 0:00 NW 3715880
Surr: n- Pentacosane 100
_0.81
0 % 20 -154 1
03112/07 0:00 NW 3715880
Prep Method Pre Da Le
Prep Initials jPrep Factor
SW3550B 03110/200715:31
JDM _- 1.00—A
)�::). 6L-"� --
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 18
B - Analyse detected in the associated Method Blank above Rep.Limit 311612a0711:01:19AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -25' Collected: 03/08/2007 16:40 SPL Sample ID: 07030504 -06
xz)
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limll(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 19
B - Analyte detected in the associated Method Blank above Rep.Limit 3/1512007 11:01:19 AM
Site: Centennial, CO
Analyses /Method
Result
QUAL MDL Rep.Llmlt DII, Factor Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 8260B
MCL
SW8260B Units: ug /kg -dry
Benzene
ND
0.12
5.8
1 03/13/0713:31
DY
3718748
Ethylbenzene
ND
D.16
5.8
1 03/13/0713:31
DY
3718748
Gasoline Range Organics
ND
11
58
1 03/13/0713:31
DY
3718748
Toluene
ND
0.2
5.8
1 03/13/0713:31
DY
3718748
Xylenes,Total
ND
0.18
5.8
1 03/13107 13:31
DY
3718748
Surr: 1,2- Dichloroethane -d4
96.7
0
k 41 -155
1 03/13/0713:31
DY
3718748
Surr: 4 Bromofluorobenzene
96.9
0
% 64 -147
1 03/13/07 13:31
DY
3718748
Surr: Toluene -d8
102
0
% 52 -152
1 03/13/07 13:31
DY
3718748
Prep Method Prep Date
jPrep Initials
Prep Factor
5W5030B _ . — 03/12/2007 15:39
IDY
11.00
xz)
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limll(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 19
B - Analyte detected in the associated Method Blank above Rep.Limit 3/1512007 11:01:19 AM
HOUSTON LABORATORY
oeor 8880 INTERCHANGE DRIVE
14060
® HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -2 -25' Collected: 03/08/2007 16:40 SPL Sample ID: 07030504 -06
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit DII. Factor Date Analyzed Analyst Seq. #
PERCENT MOISTURE MCL D2216 Units: wt%
Percent Moisture 14.4 0 0 1 03/10/07 12:17 7—L 3714712
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportabie due to Dilution
MI - Matrix Interference
* - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 20
B - Analyte detected in the associated Method Blank above Rep.Limit 311512007 11:01z20AM
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
® HOUSTON, TX 77054
(713) 660 -0901
Client Sample ID EXC -3 -10' Collected: 03/08/2007 17:00 SPL Sample ID: 07030504 -07
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limit Dil. Factor Date Analyzed Analyst Seq. #
DIESEL RANGE ORGANICS _ MCL CO_DRO Units: m !g kg-dry___
Diesel Range Organics, C11- C28 3.6 J 0.93 20 1 03/12/071:09 NW 3715957
Surr: n Pentacosane 104 0 % 20 -154 1 03/12/07 1:09 NW 3715957
Prep Method lPrep Date Prep initials Prep Factor
SW3550B M __ 03/10/2007 15:31 jJDM 11.00
D'Anna Stelly
^ : - -- -- - - - - --
Qualiflers: ND/U - Not Detected at the Method Detection Limit
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D -Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
*- Surrogate Recovery Outside Advisable QC Limits TNTC -Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 21
8 - AnWe detected in the associated Method Blank above Rep.Limit W1512007 11:01:21 AM
Client Sample ID EXC -3 -10'
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Collected: 03/08/2007 17:00 SPL Sample ID: 07030504 -07
Site: Centennial, CO
Analyses /Method Result QUAL MDL Rep.Limlt DII. Factor Date Analyzed Analyst Seq. #
VOLATILE ORGANICS BY METHOD 8260B MCL S_ W8260B Units: Itglkg -dry
Benzene 0.77 J 0.14 6.8 1 03/1310715:02 DY 3718808
Ethylbenzene
0.96
J
0.19
6.8
1
03/13/0715:02
DY
3718808
Gasoline Range Organics
32
J
13
68
1
03/13/07 15:02
DY
3718808
Toluene
3.1
J
0.23
—6-.8-
8
1
03/13/07 15:02
DY
3718808
Xylenes,Total
3.5
J
0.21
6.8
1
03113/0715:02
DY
3718808
urr:1,2- Dichloroethane -d4
93.9
0
% 41 -155
1
03/1310715:02
DY
3718608
Surr:4- BromoOuorobenzene
87.4
0
% 64 -147
1
03/1310715:02
DY
3718808
Surr: Toluene -d8
112
0
% 52 -152
1
03/13/07 15:02
DY
3718808
Prep Method Preo Date
jPpep Initials
Prep Factor
f SW5030B 7 14 43
.......... 3320... _
DY
1 00
D'Anna Stelly
Project Manager
Qualifiers: ND/U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and POL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
' - Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 22
B - Analyte detected in the associated Method Blank above Rep.Limit 311512007 1 tft21 AM
O
HOUSTON LABORATORY
8880 INTERCHANGE DRIVE
HOUSTON, TX 77054
(713) 660 -0901
Client Sample 1D EXC -3 -10' Collected: 03/08/2007 17:00 SPL Sample ID: 07030504 -07
Analyses /Method
PERCENT MOISTURE
Percent Moisture
Site: Centennial, CO
Result QUAL MDL Rep.Limit Dil. Factor Date Analyzed Analyst Seq. #1
MCL D2216 Units: wt%
26.2 0 0 1 03110/0712:45 T_L 3714731
D'Anna Stelly
Project Manager
Qualifiers: ND /U - Not Detected at the Method Detection Limit >MCL - Result Over Maximum Contamination Limit(MCL)
J - Estimated Value between MDL and PQL D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
Surrogate Recovery Outside Advisable QC Limits TNTC - Too numerous to count
E - Concentrations exceeding Calibration range of Instrument 07030504 Page 23
B - Analyte detected in the associated Method Blank above Rep.Limit 3115[2007 11:01:21 Arr